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The hydrocarbylaluminium dihalide compounds enriched in aluminium trihalide are obtained by mixing a hydrocarbylaluminium dihalide with formula AlRX2 where R is a hydrocarbyl radical containing 1 to 12 carbon atoms, such as alkyl, aryl, aralkyl, alkaryl or cycloalkyl and X is a chlorine atom or a bromine atom, with an aluminium trihalide AlX3.
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